二(2-乙基己基)磷酸酯合成路线 (共 11 条)
反应条件
sodium hydroxide in methanol; water T=100°C; 2 h; Title compound not separated from byproducts.;
参考文献
Analytical Chemistry, , vol. 78, # 5 p. 1644 - 1650
反应条件
1: sodium / 160 °C 2: nitrogen dioxide View Scheme
参考文献
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 36, p. 1853,1857; engl. Ausg. S. 1792, 1795
参考文献
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 36, p. 1853,1857; engl. Ausg. S. 1792, 1795
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <4>18, p. 287,289
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), , vol. 36, p. 1853,1857; engl. Ausg. S. 1792, 1795
反应条件
1: (chlorination) 2: aq. NaOH View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 18, p. 287 - 291
反应条件
in chloroform-d1 0.216667 h; Irradiation;
参考文献
Zhang, Youlai; Tanimoto, Hiroki; Nishiyama, Yasuhiro; Morimoto, Tsumoru; Kakiuchi, Kiyomi
Synlett, 2012 , # 3 p. 367 - 370
反应条件
P2O5 microwave irradiation;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 179, # 12 p. 2599 - 2607
反应条件
phosphorus pentoxide T=21°C; 0.616667 h; var.temps. and time; Product distributionMechanism;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 85, # 1-4 p. 91 - 100
反应条件
in tetrachloromethane; water T=29.2°C; 0.388889 h; Kinetics; Further Variations:reaction times, electrostatic field effects;
参考文献
Russian Journal of Physical Chemistry A, , vol. 82, # 3 p. 506 - 511
反应条件
sodium hydroxide in water; acetone T=20°C;
参考文献
MICHELIN RECHECHE ET TECHNIQUE S.A.
Patent: US2005/283036 A1, 2005 ;
Location in patent: Page/Page column 3 ;