4,4-二甲基-3,4-二氢-2H-萘-1-酮合成路线 （共 37 条）
反应条件
AlCl3, aluminium chloride 3 h; Heating / reflux;
参考文献
Wyeth
Patent: US2005/215539 A1, 2005 ;
Location in patent: Page/Page column 35 ;
US 20050215539 A1
反应条件
tert.-butylhydroperoxide; 4C12H25O4S(1-)*Fe2O(4+)*10H2O in water T=30°C; 50 h;
参考文献
Nagano, Takashi; Kobayashi, Shu
Chemistry Letters, 2008 , vol. 37, # 10 p. 1042 - 1043
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2 3: (i) Mg, Et2O, (ii) aq. H2SO4 4: (i) 1,1-dimethyl-propyl hydroperoxide, (ii) aq. HIO4 5: (i) PCl5, CS2, (ii) AlCl3, (iii) aq. HCl View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, # 7 p. 1663 - 1669
参考文献
Journal of Organic Chemistry, , vol. 23, p. 789,791
反应条件
1: diethyl ether; benzene; aqueous sulfuric acid 2: AlCl3 / 90 - 100 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2322,2324
反应条件
1: sulfuric acid / 0.5 h / 0 °C 2: Oxone; 2-iodo benzoic acid; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 6 h / 60 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2258 - 2265
反应条件
1: diethyl ether / 0 - 20 °C 2: sulfuric acid / 0.5 h / 0 °C 3: Oxone; 2-iodo benzoic acid; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 6 h / 60 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2258 - 2265
反应条件
1: thionyl chloride / 2 h / Reflux 2: diethyl ether / 0 - 20 °C 3: sulfuric acid / 0.5 h / 0 °C 4: Oxone; 2-iodo benzoic acid; tetra(n-butyl)ammonium hydrogensulfate / acetonitrile / 6 h / 60 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2258 - 2265
反应条件
1: SOCl2 2: (i) Mg, Et2O, (ii) aq. H2SO4 3: (i) 1,1-dimethyl-propyl hydroperoxide, (ii) aq. HIO4 4: (i) PCl5, CS2, (ii) AlCl3, (iii) aq. HCl View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, # 7 p. 1663 - 1669
反应条件
1: aqueous HCl 2: polyphosphoric acid View Scheme
参考文献
Journal of Organic Chemistry, , vol. 23, p. 789,791
