甲基-2-脱氧-L-赤式戊呋喃糖合成路线 （共 38 条）
反应条件
bis-(1,2-dimethylpropyl)borane 24 h; Ambient temperature;
参考文献
Murakami, Masahiro; Mukaiyama, Teruaki
Chemistry Letters, 1982 , p. 241 - 244
反应条件
ethylenediaminetetraacetic acid in water 48 h; deoxyribose-5-phosphate aldolase (DERA), phosphate buffer, pH 7.3;
参考文献
Chen, Lihren; Dumas, David P.; Wong, Chi-Huey
Journal of the American Chemical Society, 1992 , vol. 114, # 2 p. 741 - 748
反应条件
water T=20°C; Acidic aqueous solution;
参考文献
US2006/205685 A1, ;
Page/Page column 4; sheet 3 ;
反应条件
acetic acid in tetrahydrofuran; water T=60 - 70°C; 24 h;
参考文献
Yamamoto, Yoshihiro; Kirihata, Mitsunori; Ichimoto, Itsuo; Ueda, Hiroo
Agricultural and Biological Chemistry, 1985 , vol. 49, # 5 p. 1435 - 1440
反应条件
1: CF3COOH / H2O / 2 h / Ambient temperature 2: imidazole / dimethylformamide / 3 h / Ambient temperature 3: 90.4 percent / DIBAL / toluene / 0.25 h / -78 °C 4: 62 percent / AcOH / tetrahydrofuran; H2O / 24 h / 60 - 70 °C View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 49, # 5 p. 1435 - 1440
反应条件
1: 1.) 10percent sodium hydroxide / 1.) EtOH 2: trifluoroacetic acid / H2O 3: bis(3-methyl-2-butyl)borane / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 21 p. 5788 - 5789
反应条件
potassium phosphate buffer; magnesium sulfate in water; xylene T=47°C; pH=7.0; 22 h; Enzymatic reaction;
参考文献
Bioscience, Biotechnology and Biochemistry, , vol. 70, # 6 p. 1371 - 1378
反应条件
1: Butadiene monooxide With 3,3-dimethyldioxirane in acetone T=-15°C; 2.5 h; 2: L-2'-deoxyguanosine in acetic acid T=60°C; 22 h; 3: With hydrogenchloride T=80°C; 2.5 h;
参考文献
Chemical Research in Toxicology, , vol. 12, # 3 p. 247 - 257
反应条件
hydrogenchloride; water T=100°C; 48 h;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 20 p. 6460 - 6470
反应条件
hydrogenchloride 1.) 2-deoxyribose-5-phospatte aldolase, triose phosphate isomerase, pH=7.3, 6 d, 2.) acid phosphatase, 37 deg C, pH=4.7, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 117, # 29 p. 7585 - 7591
