2-甲基-3-丁炔-2-胺合成路线 （共 36 条）
反应条件
sodium amide in diethyl ether; ammonia
参考文献
Kopka, Ihor E.; Fataftah, Zacharia A.; Rathke, Michael W.
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4616 - 4622
反应条件
lithium amide in ammonia T=-33°C; 1 h;
参考文献
Geri, Roberto; Polizzi, Carmela; Lardicci, Luciano; Caporusso, Anna Maria
Gazzetta Chimica Italiana, 1994 , vol. 124, # 6 p. 241 - 248
反应条件
trifluoroacetic acid in dichloromethane T=20°C; 0.5 h;
参考文献
Rajagopal, Basker; Chen, Ying-Yu; Chen, Chun-Chi; Liu, Xuan-Yu; Wang, Huei-Ren; Lin, Po-Chiao
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1254 - 1264
反应条件
1: 30 percent / calcium chloride, Cu2Cl2 (95percent brown powder). copper bronze powder, conc. HCl / 1 h / 0 - 5 °C 2: 42 percent / sodamide / liquid ammonia; diethyl ether View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4616 - 4622
参考文献
Alhalib, Ali; Moran, Wesley J.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 5 p. 795 - 800
反应条件
1: Cu, aq. KOH 2: HCO2H View Scheme
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
反应条件
potassium hydroxide; hydrogen; Pd/BaCO3 in pentane
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
反应条件
1: H2 / Raney-Ni / ethanol 2: Cu, aq. KOH View Scheme
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Alhalib, Ali; Moran, Wesley J.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 5 p. 795 - 800
反应条件
1: H2 / Raney-Ni / ethanol 2: Cu, aq. KOH 3: Na, liq. NH3, NH4Cl View Scheme
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
