1-(甲磺酰基)-4-硝基苯合成路线 (共 34 条)
反应条件
potassium permanganate; manganese sulphate T=20°C; 0.5 h;
参考文献
Yang, Chuanbo; Jin, Qingping; Zhang, Hua; Liao, Jian; Zhu, Jin; Yu, Bin; Deng, Jingen
Green Chemistry, 2009 , vol. 11, # 9 p. 1401 - 1405
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=0°C; 2 h;
参考文献
F2G LTD
Patent: WO2006/123145 A1, 2006 ;
Location in patent: Page/Page column 52 ;
反应条件
(S)-(-)-2-(N-3,5-diiodosalicylidene)amino-3,3-dimethyl-1-butanol; dihydrogen peroxide; p-methoxybenzoic acid Li-salt; Fe(acac)3 in dichloromethane; water T=20°C; 16 h;
参考文献
Legros, Julien; Bolm, Carsten
Chemistry - A European Journal, 2005 , vol. 11, # 4 p. 1086 - 1092
反应条件
3-chloro-benzenecarboperoxoic acid in 1,2-dichloro-ethane 10 h; Reflux;
参考文献
Liu, Jia; Li, Jue; Ren, Jiangmeng; Zeng, Bu-Bing
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1581 - 1584
反应条件
urea hydrogen peroxide; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=0°C; Electrochemical reaction;
参考文献
Tetrahedron Letters, , vol. 49, # 39 p. 5611 - 5613
反应条件
4-(N,N-dimethlyamino)pyridine; iodosylbenzene; 2C24H20B(1-)*C55H58Mn2N4O9(2+) in acetonitrile T=20°C; 2 h; optical yield given as percent eeenantioselective reaction;
参考文献
Hirotsu, Masakazu; Ohno, Naoki; Nakajima, Takashi; Kushibe, Chie; Ueno, Keiji; Kinoshita, Isamu
Dalton Transactions, 2010 , vol. 39, # 1 p. 139 - 148
反应条件
m-chloro-peroxy-benzoic acid in chloroform; ethyl acetate
参考文献
Eli Lilly and Company
Patent: US6635657 B1, 2003 ;
US 6635657 B1
反应条件
copper(l) iodide in dimethyl sulfoxide 32 h; Heating;
参考文献
Bian, Ming; Xu, Fada; Ma, Cheng
Synthesis, 2007 , # 19 p. 2951 - 2956
反应条件
2-methyl-cyclopentanone; benzylamine in acetic acid 2 h; Heating;
参考文献
Reddy, Moole Venkata Ramana; Reddy, Sirigiri; Reddy, Dandu Bhaskar; Seenaiah, Biradavolu
Acta Chimica Hungarica, 1989 , vol. 126, # 6 p. 825 - 828
反应条件
1: With bis(acetylacetonate)oxovanadium; (R)-diiodo Shiff base ligand in chloroform T=22°C; 1 h; 2: With dihydrogen peroxide in chloroform T=22°C; 20 h; Title compound not separated from byproducts;
参考文献
Synlett, , # 20 p. 3540 - 3544