2,2'-[(4-氟-3-硝基苯基)亚氨基]双乙醇合成路线 （共 3 条）
反应条件
1.1: water / 4.5 h / 70 °C 2.1: hydrogen; / ethanol / 2 h / 23 °C / 2585.81 - 3102.97 Torr / |Inert atmosphere 3.1: ethanol / 5 h / 23 °C / 2585.81 - 3102.97 Torr / |Inert atmosphere 4.1: hydrogenchloride / water; methyl acetate / 2.5 h / 73 °C 4.2: pH 6.0 View Scheme
参考文献
SYNTHON BV; BARTOS, Petr; BENOVSKY, Petr; BARTL, Jiri
Patent: WO2013/150020 A1, 2013 ;
反应条件
1: water / 4.5 h / 70 °C 2: hydrogen; / ethanol / 2 h / 23 °C / 2585.81 - 3102.97 Torr / |Inert atmosphere 3: ethanol / 5 h / 23 °C / 2585.81 - 3102.97 Torr / |Inert atmosphere 4: hydrogenchloride / water / 2.5 h / 60 °C / pH Ca. 2 View Scheme
参考文献
SYNTHON BV; BARTOS, Petr; BENOVSKY, Petr; BARTL, Jiri
Patent: WO2013/150020 A1, 2013 ;
反应条件
in water T=70°C; 4.5 h; Reagent/catalystTime;
参考文献
SYNTHON BV; BARTOS, Petr; BENOVSKY, Petr; BARTL, Jiri
Patent: WO2013/150020 A1, 2013 ;
Location in patent: Page/Page column 17 ;
