2,3,4-三(苄氧基)-6,8-二氧杂双环[3.2.1]辛烷合成路线 (共 9 条)
反应条件
silica-supported perchloric acid in acetonitrile T=70°C; 0.0833333 h; Inert atmosphere;
参考文献
Chun, Yuexing; Yan, Shiqiang; Li, Xiangpeng; Ding, Ning; Zhang, Wei; Wang, Peng; Li, Ming; Li, Yingxia
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6196 - 6198
反应条件
silica-supported perchloric acid in acetonitrile T=70°C; 0.0333333 h; Inert atmosphere;
参考文献
Chun, Yuexing; Yan, Shiqiang; Li, Xiangpeng; Ding, Ning; Zhang, Wei; Wang, Peng; Li, Ming; Li, Yingxia
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6196 - 6198
反应条件
silica-supported perchloric acid in acetonitrile T=70°C; 0.0333333 h; Inert atmosphere;
参考文献
Chun, Yuexing; Yan, Shiqiang; Li, Xiangpeng; Ding, Ning; Zhang, Wei; Wang, Peng; Li, Ming; Li, Yingxia
Tetrahedron Letters, 2011 , vol. 52, # 46 p. 6196 - 6198
反应条件
Fe(ClO4)3*6H2O in acetonitrile T=80°C; 5 h;
参考文献
UNIVERSITY COLLEGE DUBLIN, NATIONAL UNIVERSITY OF IRELAND, DUBLIN
Patent: US2010/184711 A1, 2010 ;
Location in patent: Figure 1 ;
反应条件
AuBr3 in acetonitrile T=70°C; 12 h; Inert atmosphere;
参考文献
Thadke, Shivaji A.; Hotha, Srinivas
Tetrahedron Letters, 2010 , vol. 51, # 45 p. 5912 - 5914
反应条件
zirconocene dichloride; silver perchlorate in diethyl ether T=20°C; 20 h; Yields of byproduct given;
参考文献
Murakata, Chikara; Ogawa, Tomoya
Carbohydrate Research, 1992 , vol. 235, p. 95 - 114
反应条件
sodium hydride 1) DMF, 2) DMF, 4 h; Yield given. Multistep reaction;
参考文献
Paulsen, Hans; Lockhoff, Oswald
Chemische Berichte, 1981 , vol. 114, # 9 p. 3079 - 3101
反应条件
palladium on activated charcoal in isopropyl alcohol 5 h; Heating;
参考文献
Cruzado, M. Carmen; Martin-Lomas, Manuel
Carbohydrate Research, 1987 , vol. 170, p. 249 - 254
反应条件
palladium on activated charcoal in isopropyl alcohol 5 h; Heatingfurther O-benzyl protecting 1,6-anhydrohexoses, various reaction time;
参考文献
Tetrahedron Letters, , vol. 27, # 22 p. 2497 - 2500