1,4-苯并二恶烷-6-甲醛合成路线 （共 44 条）
反应条件
1: With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 4 h;
2: With water in N,N-dimethyl-formamide
4 h; Acidic conditions;
参考文献
Cheng, Huicheng; Pei, Yu; Leng, Faqiang; Li, Jingya; Liang, Apeng; Zou, Dapeng; Wu, Yangjie; Wu, Yusheng
Tetrahedron Letters, 2013 , vol. 54, # 33 p. 4483 - 4486
反应条件
bromine in acetic acid
T=0°C;
参考文献
Guillaumet, G.; Hretani, M.; Coudert, G.
Tetrahedron Letters, 1988 , vol. 29, # 22 p. 2665 - 2666
反应条件
1: With sodium hydroxide in methanol
T=20°C; 1 h;
2: With sodium tetrahydroborate in methanol
T=0 - 20°C; 1 h;
参考文献
ANALYTECON SA
Patent: WO2007/29106 A1, 2007 ;
Location in patent: Page/Page column 38 ;
WO 2007/029106 A1
反应条件
potassium hydroxide in ethanol; water
T=0 - 20°C; Claisen Schmidt condensation;
参考文献
Khalilullah, Habibullah; Khan, Shamshir; Ahsan, Mohamed Jawed; Ahmed, Bahar
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 24 p. 7251 - 7254
