Titanium(IV) oxide; trifluoroacetic acid in acetonitrile
24 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Lai; Mallouk
Journal of the Chemical Society - Series Chemical Communications, 1993 , # 17 p. 1359 - 1361
Anderson, H. H.; Stanislov, G. N.
Journal of Organic Chemistry, 1953 , vol. 18, p. 1716 - 1721
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Gmelin Handbook: Si: MVol.C, 69, page 190 - 194
in neat (no solvent)
under inert atm. mixt. Bi and CF3COOAg in evacuated Pyrex ampule was placed in electric furnace having temp. gradient along the length of tube and kept at 110°C for 4 days;
参考文献
Dikarev, Evgeny V.; Li, Bo
Inorganic Chemistry, 2004 , vol. 43, # 11 p. 3461 - 3466
in water
Ag2C2 added to aq. soln. of AgCF3COO with stirring, filtered, org. compd. added to filtrate; filtered, allowed to stand without disturbance for several d, elem. anal.;
参考文献
Wang, Quan-Ming; Lee, Hung Kay; Mak, Thomas C. W.
New Journal of Chemistry, 2002 , vol. 26, # 5 p. 513 - 515
