2,4,6-三甲基苯基异氰酸酯合成路线 (共 32 条)
反应条件
tributylphosphine; di-isopropyl azodicarboxylate in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Saylik, Dilek; Horvath, Michael J.; Elmes, Patricia S.; Jackson, W. Roy; Lovel, Craig G.; Moody, Keith
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3940 - 3946
反应条件
triphenylphosphine in dichloromethane T=-78 - 20°C; P=760 Torr;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3940 - 3946
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 0.166667 h;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias; Schlechtingen, Georg
Angewandte Chemie, 1995 , vol. 107, # 22 p. 2746 - 2749
反应条件
(Bu4N)lt;PdCl3(CO)gt;; cocatalyst VOCl2*2THF in 1,2-dichloro-benzene T=100°C; P=750.06 Torr; other catalysts and other cocatalysts; Product distributionRate constant;
参考文献
Tietz, Helmuth; Schwetlick, Klaus; Kreisel, Guenter
Zeitschrift fuer Chemie (Stuttgart, Germany), 1985 , vol. 25, # 8 p. 290 - 291
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=82°C; 18 h;
参考文献
Angewandte Chemie, , vol. 107, # 22 p. 2746 - 2749
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=25°C; 4 h;
参考文献
Angewandte Chemie, , vol. 107, # 22 p. 2746 - 2749
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in dimethyl sulfoxide Ambient temperature;
参考文献
Braverman; Cherkinsky; Kedrova; Reiselman
Tetrahedron Letters, 1999 , vol. 40, # 16 p. 3235 - 3238
反应条件
2: 75 percent / DBU / dimethylsulfoxide / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 16 p. 3235 - 3238
反应条件
in benzene 3 h; Heating;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1212
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1339 - 1340
反应条件
in benzene 3 h; Heating;
参考文献
Vovk, M. V.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 6 p. 1212
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 6 p. 1339 - 1340