2,2-二甲基-1,3-二氯丙烷合成路线 (共 4 条)
反应条件
thionyl chloride; triphenyl-phosphine oxide T=20 - 115°C; 9.5 h;
参考文献
BASF SE
Patent: US2008/228016 A1, 2008 ;
Location in patent: Page/Page column 5 ;
反应条件
chlorine in 1,2,2-trifluoro-trichloroethane T=23°C; Irradiationvar. neopentane conc., solvents, solvents mixtures, and in vapour phase; other alkanes; MechanismProduct distribution;
参考文献
Journal of the American Chemical Society, , vol. 113, # 14 p. 5397 - 5402
反应条件
1: chloro-diphenylphosphine With sodium in anhydrous butyl ether
T=130°C;
2: 1,3-dichloro-2,2-dimethyl propane in anhydrous butyl ether
T=130°C;
参考文献
BASF Aktiengesellschaft
Patent: WO2006/84878 A1, 2006 ;
Location in patent: Page/Page column 21 ;
反应条件
chlorine in chloroform
50 h; Irradiation;
参考文献
Dehmlow,E.V.; Hoefle,G.
Chemische Berichte, 1974 , vol. 107, p. 2760 - 2767