3,7,11-三甲基-2,6,10-十二烷三烯-1-醇乙酸酯合成路线 （共 5 条）
反应条件
1: farnesyl benzoate With sodium methylate T=20°C; 2: methyl acetate T=50°C; 3 h;
参考文献
BASF SE
Patent: US2010/222606 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
darauffolgende Verseifung durch Erwaermen mit methylalkoholischer Alkalilauge.Hydrogenation;
参考文献
Fischer,F.G.
Justus Liebigs Annalen der Chemie, 1928 , vol. 464, p. 82,86
反应条件
1: (i) H2, Pd-CaCO3, (ii) (hydrolysis) 2: H2SO4, aq. HBr / Heating 3: (i) Mg, (ii) /BRN= 1634534/, (iii) KHSO4 4: (hydrogenation) 5: (i) nBuLi, (ii) /BRN= 1724987/, (iii) H2 View Scheme
参考文献
Journal of the Chemical Society, , p. 5706 - 5713
反应条件
1: (i) H2, Pd-CaCO3, (ii) (hydrolysis) 2: KOH / 260 °C View Scheme
参考文献
Johnstone,R.A.W.; Quan,P.M.
Journal of the Chemical Society, 1963 , p. 5706 - 5713
反应条件
1: (i) H2, Pd-CaCO3, (ii) (hydrolysis)
2: H2SO4, aq. HBr / Heating
3: KOH, EtOH / Heating
View Scheme
参考文献
Johnstone,R.A.W.; Quan,P.M.
Journal of the Chemical Society, 1963 , p. 5706 - 5713
