反应条件
1: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, from 50 to 55 deg C, 60 min, 2.) THF, a) -78 deg C, 30 min, b) 20 deg C, 12 h 2: 82 percent / LiAlH4 / diethyl ether / 5 h / 20 °C 3: 67 percent / pyridinium chlorochromate / CH2Cl2 / 0.67 h / 20 °C View Scheme
参考文献
Dzhumakulov, T.; Kadyrova, M. M.
Chemistry of Natural Compounds, 1992 , vol. 28, # 2 p. 240 - 241
Khimiya Prirodnykh Soedinenii, 1992 , # 2 p. 276 - 277
