1,4,7,10-四氮环十四烷合成路线 （共 6 条）
反应条件
1: With potassium carbonate in acetonitrile 2: With hydrazine hydrate
参考文献
Ruloff, Robert; Toth, Eva; Scopelliti, Rosario; Tripier, Raphael; Handel, Henri; Merbach, Andre E.
Chemical Communications, 2002 , # 22 p. 2630 - 2631
反应条件
1: 90 percent / ethanol / 3 h / 0 °C 2: 55 percent / cesium carbonate / acetonitrile / 96 h / 40 °C 3: hydrochloric acid / H2O / 6 h / 60 °C View Scheme
参考文献
Prokhorov, Anton; Le Bris, Nathalie; Bernard, Helene; Claudon, Geraldine; Handel, Henri
Synthetic Communications, 2006 , vol. 36, # 21 p. 3271 - 3282
反应条件
1: 90 percent / ethanol / 3 h / 0 °C 2: 56 percent / cesium carbonate / acetonitrile / 48 h / 40 °C 3: hydrochloric acid / H2O / 6 h / 60 °C View Scheme
参考文献
Prokhorov, Anton; Le Bris, Nathalie; Bernard, Helene; Claudon, Geraldine; Handel, Henri
Synthetic Communications, 2006 , vol. 36, # 21 p. 3271 - 3282
参考文献
Fabbrizzi, Luigi; Micheloni, Mauro; Paoletti, Piero
Inorganic Chemistry, 1980 , vol. 19, p. 535 - 538
参考文献
Fabbrizzi, Luigi; Micheloni, Mauro; Paoletti, Piero
Inorganic Chemistry, 1980 , vol. 19, p. 535 - 538
反应条件
1: K2CO3 / acetonitrile
2: aq. HCl
View Scheme
参考文献
Ruloff, Robert; Toth, Eva; Scopelliti, Rosario; Tripier, Raphael; Handel, Henri; Merbach, Andre E.
Chemical Communications, 2002 , # 22 p. 2630 - 2631
