4-甲氧基-3,5-二硝基甲苯合成路线 （共 17 条）
反应条件
toluene T=120 - 140°C;
参考文献
Chemische Berichte, , vol. 70, p. 2396,2400
反应条件
sulfuric acid; nitric acid
参考文献
American Chemical Journal, , vol. 19, p. 536
反应条件
nitric acid; acetic anhydride T=0°C; 1 h;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 1233 - 1240
反应条件
nitric acid; acetic anhydride; trifluoroacetic anhydride T=-20°C; 0.5 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 1233 - 1240
反应条件
1: 76 percent / aq. NaOH / 3 h / Heating 2: nitric acid, Ac2O, trifluoroacetic anhydride / 0.5 h / -20 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 1233 - 1240
反应条件
nitric acid; trifluoroacetic anhydride T=-20°C; 0.5 h; Further byproducts given;
参考文献
Canadian Journal of Chemistry, , vol. 65, p. 1233 - 1240
反应条件
1: Diazotization.Zersetzung des Reaktionsprodukts mit Methylalkohol 2: sulfuric acid; concentrated nitric acid View Scheme
参考文献
American Chemical Journal, , vol. 19, p. 536
反应条件
(i) NaOH, (ii) benzene; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 39, p. 3165 - 3167
参考文献
Journal of Organic Chemistry, , vol. 38, # 6 p. 1204 - 1206
参考文献
Justus Liebigs Annalen der Chemie, , vol. 217, p. 172
Chemische Berichte, , vol. 56, p. 1490
