反应条件
lithium in tetrahydrofuran byproducts: (MePhHSi)2; a trace amt. of Li and equiv. amt. of neo-penthyl chloride in ether after 12 h were added to silane, room temp., 24 h, N2 atm.; hydrolysis, extn. (ether), evapn., not sep. detected with NMR and GLC;
参考文献
Corriu, R. J. P.; Ould-Kada, S.; Lanneau, G. F.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 39 - 50