2,3-二氯二苯并-对-二恶英合成路线 （共 8 条）
反应条件
copper(ll) bromide T=260 - 300°C; Chlorination; bromination; 0.166667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Jay; Stieglitz
Chemosphere, 1997 , vol. 35, # 5 p. 987 - 991
反应条件
potassium 1) HMPA, 20 deg C; 2) 110 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.; Rembovskii, V. R.; Troshkin, N. M.; Baulin, S. I.
Doklady Chemistry, 1993 , vol. 332, # 4 p. 225 - 229
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 332, # 4 p. 461 - 465
反应条件
acetophenone in methanol T=20°C; 3 h; Irradiation;
参考文献
Kobayashi, Takanori; Shimada, Jun-Ichi; Kitahara, Chieko; Haga, Naoki
Chemistry Letters, 2006 , vol. 35, # 4 p. 348 - 349
反应条件
1: 55.9 percent / acetophenone / methanol / 3 h / 20 °C / Irradiation 2: 95.7 percent / acetophenone / methanol / 0.17 h / 20 °C / Irradiation View Scheme
参考文献
Kobayashi, Takanori; Shimada, Jun-Ichi; Kitahara, Chieko; Haga, Naoki
Chemistry Letters, 2006 , vol. 35, # 4 p. 348 - 349
反应条件
nitric acid in acetic acid
1 h; Heating;
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Chernov, S. A.
Russian Journal of General Chemistry, 1993 , vol. 63, # 8.2. p. 1279 - 1286
Zhurnal Obshchei Khimii, 1993 , vol. 63, # 8 p. 1831 - 1842
反应条件
1: 97 percent / nitric acid / acetic acid / 1 h / Heating
2: 58 percent / SnCl2*2H2O / ethanol; aq. HCl / Heating
3: 87 percent / acetic acid / 1 h / 90 - 100 °C
4: 59 percent / Cl2 / dioxane / 0.5 h / 40 °C
5: 91 percent / EtOH, Na / 0.25 h / Heating
View Scheme
参考文献
Kuntsevich, A. D.; Golovkov, V. F.; Rembovskii, V. R.; Chernov, S. A.
Doklady Chemistry, 1993 , vol. 330, # 1-3 p. 133 - 136
Dokl. Akad. Nauk SSSR Ser. Khim., 1993 , vol. 330, # 3 p. 333 - 336
反应条件
acetophenone in methanol
T=20°C; 3 h; Irradiation;
参考文献
Kobayashi, Takanori; Shimada, Jun-Ichi; Kitahara, Chieko; Haga, Naoki
Chemistry Letters, 2006 , vol. 35, # 4 p. 348 - 349
反应条件
in methanol
T=20°C; 0.166667 h; Irradiation;
参考文献
Kobayashi, Takanori; Shimada, Jun-Ichi; Kitahara, Chieko; Haga, Naoki
Chemistry Letters, 2006 , vol. 35, # 4 p. 348 - 349
