(S)-5-羟基-7,4'-二甲氧基黄烷酮合成路线 （共 16 条）
反应条件
ethylenediaminetetraacetic acid; 1,4-dithio-DL-threitol; naringenin 7-O-methyltransferase GST recombinant T=30°C; 0.0833333 h; aq. bufferEnzymatic reaction; Kinetics;
参考文献
Shimizu, Takafumi; Lin, Fengqiu; Hasegawa, Morifumi; Okada, Kazunori; Nojiri, Hideaki; Yamane, Hisakazu
Journal of Biological Chemistry, 2012 , vol. 287, # 23 p. 19315 - 19325
反应条件
4-methylmorpholine N-oxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dimethyl sulfoxide T=20°C; 48 h;
参考文献
Righi, Giuliana; Silvestri, Ilaria Proietti; Barontini, Maurizio; Crisante, Fernanda; Di Manno, Andrea; Pelagalli, Romina; Bovicelli, Paolo
Natural Product Research, 2012 , vol. 26, # 14 p. 1278 - 1284
反应条件
1.1: 4-methylmorpholine N-oxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 48 h / 20 °C 2.1: tetra-n-butylammonium tribromide / chloroform / 1.33 h / 20 °C 3.1: sodium methylate; copper(I) bromide / N,N-dimethyl-formamide / 1 h / 20 °C 3.2: 5 h / 120 °C View Scheme
参考文献
Righi, Giuliana; Silvestri, Ilaria Proietti; Barontini, Maurizio; Crisante, Fernanda; Di Manno, Andrea; Pelagalli, Romina; Bovicelli, Paolo
Natural Product Research, 2012 , vol. 26, # 14 p. 1278 - 1284
反应条件
1.1: 4-methylmorpholine N-oxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 48 h / 20 °C 2.1: tetra-n-butylammonium tribromide / chloroform / 1.33 h / 20 °C 3.1: sodium methylate; copper(I) bromide / N,N-dimethyl-formamide / 1 h / 20 °C 3.2: 5 h / 120 °C 4.1: hydrogen bromide; acetic acid / water View Scheme
参考文献
Righi, Giuliana; Silvestri, Ilaria Proietti; Barontini, Maurizio; Crisante, Fernanda; Di Manno, Andrea; Pelagalli, Romina; Bovicelli, Paolo
Natural Product Research, 2012 , vol. 26, # 14 p. 1278 - 1284
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethyl acetate 4 h; Ambient temperature;
参考文献
Kamiya, Shintaro; Esaki, Sachiko; Shiba, Naoko; Hoshi, Takeshi
Agricultural and Biological Chemistry, 1989 , vol. 53, # 5 p. 1365 - 1374
反应条件
1: H2 / Pd-C / ethanol
2: methanol; diethyl ether
View Scheme
参考文献
Nilsson,M.
Acta Chemica Scandinavica (1947-1973), 1961 , vol. 15, p. 154 - 158
