3-(3-甲基-苯基)丙酸甲酯合成路线 （共 9 条）
反应条件
hydrogen; palladium on activated charcoal in methanol 1 h; Ambient temperature;
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
1: NaOCH3 / CH2Cl2 / Ambient temperature 2: H2 / 5percent Pd/C / methanol / 1 h / Ambient temperature View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
sulfuric acid Heating;
参考文献
Bohman; Nordlander; Nordenhem; Sunnerheim; Borg-Karlson; Unelius
Journal of Chemical Ecology, 2008 , vol. 34, # 3 p. 339 - 352
反应条件
Rh(I)Cl(CO)(PMe3)2 8 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sasaki, Koushi; Sakakura, Toshiyasu; Tokunaga, Yuko; Wada, Keisuke; Tanaka, Masato
Chemistry Letters, 1988 , p. 685 - 688
反应条件
Rh(I)Cl(CO)(PMe3)2 8 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sasaki, Koushi; Sakakura, Toshiyasu; Tokunaga, Yuko; Wada, Keisuke; Tanaka, Masato
Chemistry Letters, 1988 , p. 685 - 688
反应条件
Rh(I)Cl(CO)(PMe3)2 8 h; Ambient temperatureIrradiation; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Sasaki, Koushi; Sakakura, Toshiyasu; Tokunaga, Yuko; Wada, Keisuke; Tanaka, Masato
Chemistry Letters, 1988 , p. 685 - 688
反应条件
(i) (catalytic hydrogenation), (ii) /BRN= 1098229/, H2SO4; Multistep reaction;
参考文献
Meyer,A. et al.
Chemische Berichte, 1977 , vol. 110, p. 1403 - 1420
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
反应条件
1: LiAlH4 / diethyl ether / 1 h / Heating
2: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -40 deg C, 25 min, 2.) CH2Cl2, -40 deg C, 5 min
View Scheme
参考文献
Hashizume; Ito; Yamada; Nagashima; Kanao; Tomoda; Sunazuka; Kumagai; Omura
Chemical and pharmaceutical bulletin, 1994 , vol. 42, # 3 p. 512 - 520
