2-甲基-5-甲氧基苯并噻唑合成路线 （共 14 条）
反应条件
1: With copper(l) iodide; K2S in N,N-dimethyl-formamide T=140°C; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C;
参考文献
Ma, Dawei; Xue, Peng; Jiang, Yongwen; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua
Angewandte Chemie, International Edition, 2009 , vol. 48, # 23 p. 4222 - 4225
反应条件
t-Bu Brett Phos; C44H62NO5PPdS; sodium t-butanolate in 1,4-dioxane T=80°C; 20 h; Sealed tubeInert atmosphere;
参考文献
Cheung, Chi Wai; Buchwald, Stephen L.
Organic Letters, 2013 , vol. 15, # 15 p. 3998 - 4001
反应条件
acetic acid; zinc anschliessendes Erhitzen mit Acetanhydrid;
参考文献
Sweschnikow; Lewkoew
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1071,1072, 1073
Chem.Abstr., 1947 , p. 2734
反应条件
sodium hydroxide; potassium hexacyanoferrate(III)
参考文献
Sweschnikow; Lewkoew
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1071,1072, 1073
Chem.Abstr., 1947 , p. 2734
反应条件
1: ethanol; sodium polysulfide 2: zinc-powder; acetic acid / anschliessendes Erhitzen mit Acetanhydrid View Scheme
参考文献
Sweschnikow; Lewkoew
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1071,1072, 1073
Chem.Abstr., 1947 , p. 2734
反应条件
1: benzene; phosphorus (V)-sulfide 2: K3<Fe(CN)6>; aqueous NaOH View Scheme
参考文献
Sweschnikow; Lewkoew
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1071,1072, 1073
Chem.Abstr., 1947 , p. 2734
参考文献
Mizuno et al.
Yakugaku Zasshi, 1956 , vol. 76, p. 329,332
Chem.Abstr., 1956 , p. 13878
参考文献
Fitton; Hatton; Ward
Journal of the Chemical Society. Perkin transactions 1, 1970 , vol. 11, p. 1553 - 1556
反应条件
T=80 - 100°C; anschliessendes Erhitzen mit Acetanhydrid auf 114-117grad;
参考文献
Sweschnikow; Lewkoew
Zhurnal Obshchei Khimii, 1946 , vol. 16, p. 1071,1072, 1073
Chem.Abstr., 1947 , p. 2734
反应条件
sodium hydroxide in ethylene glycol 3 h; Heating;
参考文献
Hodson, Stephen J.; Bishop, Michael J.; Speake, Jason D.; Navas III, Frank; Garrison, Deanna T.; Bigham, Eric C.; Saussy Jr., David L.; Liacos, James A.; Irving, Paul E.; Jeffrey Gobel; Sherman, Bryan W.
Journal of Medicinal Chemistry, 2002 , vol. 45, # 11 p. 2229 - 2239
