1-氨基-2-氰基-1-环戊烯合成路线 （共 16 条）
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78 - -20°C;
参考文献
Rodriguez-Hahn, Lydia; Parra M., Margarita; Martinez, Mariano
Synthetic Communications, 1984 , vol. 14, # 10 p. 967 - 972
反应条件
ammonia; hydrogen; iron catalyst, based on magnetite ore and prepared according to Example 2 (a) of DE 19636767 T=30 - 340°C; 1524 h; Compressed gas(es); Conversion of starting material;
参考文献
BASF Aktiengesellschaft
Patent: US6346641 B1, 2002 ;
Location in patent: Page column 7 ;
反应条件
1: P2O5 / 110 - 125 °C 2: ethyl magnesium bromide; diethyl ether View Scheme
参考文献
Compere
Bulletin des Societes Chimiques Belges, 1935 , vol. 44, p. 524
反应条件
1: alcohol; sodium cyanoacetic ester 2: aqueous KOH-solution / 50 °C View Scheme
参考文献
Best; Thorpe
Journal of the Chemical Society, 1909 , vol. 95, p. 705
反应条件
sodium hydroxide in methanol; ethanol; water; cyclohexanone; toluene
参考文献
Nikken Chemicals Co., Ltd.
Patent: US6433173 B1, 2002 ;
反应条件
zinc(II) chloride in xylene Heating;
参考文献
Goncharenko, S. B.; Kaganskii, M.M.; Portnov, Yu. N.; Granik, V. G.
Pharmaceutical Chemistry Journal, 1992 , vol. 26, # 9-10 p. 769 - 772
Khimiko-Farmatsevticheskii Zhurnal, 1992 , vol. 26, # 9-10 p. 83 - 85
反应条件
pyridine 16 h; Reflux;
参考文献
Ma, Miaofeng; Hou, Guohua; Wang, Junru; Zhang, Xumu
Tetrahedron Asymmetry, 2011 , vol. 22, # 5 p. 506 - 511
反应条件
sodium hydroxide in toluene
参考文献
Schelhaas, Michael; Jautelat, Manfred
Patent: US2002/7081 A1, 2002 ;
反应条件
sodium hydroxide in toluene
参考文献
Schelhaas, Michael; Jautelat, Manfred
Patent: US2002/7081 A1, 2002 ;
反应条件
hydrogenchloride 4 h; Ambient temperature;
参考文献
Coates,R.M.; Rogers,B.D.; Hobbs,S.J.
Journal of the American Chemical Society, 1987 , vol. 109, p. 1160
