1,4,7,10-四氮杂环十二烷合成路线 (共 64 条)
参考文献
Oliver, Morag; Jorgensen, Michael R.; Miller, Andrew D.
Synlett, 2004 , # 3 p. 453 - 456
反应条件
1: 95 percent / H2O; methanol / 3 h / 20 °C 2: 90 percent / acetonitrile / 24 h / 20 °C 3: 85 percent / hydrazine monohydrate / 120 °C View Scheme
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
in chloroform T=20°C;
参考文献
Fujioka, Haruto; Kishida, Sayuri; Ishizu, Takashi; Shiro, Motoo; Kinoshita, Eiji; Koike, Tohru
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 3 p. 267 - 272
反应条件
Yield given. Multistep reaction;
参考文献
Yaouanc, Jean-Jacques; Bris, Nathalie Le; Gall, Guenaelle Le; Clement, Jean-Claude; Handel, Henri; Abbayes, Herve des
Journal of the Chemical Society, Chemical Communications, 1991 , # 4 p. 206 - 207
反应条件
in chloroform T=20°C; 1 h;
参考文献
Waengler, Bjoern; Beck, Carmen; Wagner-Utermann, Ulrike; Schirrmacher, Esther; Bauer, Claudia; Roesch, Frank; Schirrmacher, Ralf; Eisenhut, Michael
Tetrahedron Letters, 2006 , vol. 47, # 33 p. 5985 - 5988
反应条件
triethylamine in methanol; dichloromethane 12 - 16 h;
参考文献
SEMAFORE PHARMACEUTICALS INC.
Patent: WO2005/32599 A1, 2005 ;
Location in patent: Page/Page column 22-24; figure 12 ;
反应条件
in chloroform T=0 - 20°C;
参考文献
Chong, Hyun-Soon; Lim, Sooyoun; Baidoo, Kwamena E.; Milenic, Diane E.; Ma, Xiang; Jia, Fang; Song, Hyun A.; Brechbiel, Martin W.; Lewis, Michael R.
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 21 p. 5792 - 5795
反应条件
in acetonitrile Heating; Yield given;
参考文献
Anelli; Murru; Uggeri; Virtuani
Journal of the Chemical Society - Series Chemical Communications, 1991 , # 18 p. 1317 - 1318
反应条件
1: dimethylformamide / Ambient temperature 2: K2CO3, TBACl / dimethylformamide / 2 h / Ambient temperature 3: 0.28 g / TFA / 0 °C View Scheme
参考文献
Grierson, John R.; Shoner, Steven C.; Eary, Janet F.
Journal of Labelled Compounds and Radiopharmaceuticals, 1997 , vol. 40, p. 512 - 514
反应条件
triethylamine in chloroform
参考文献
Liu, Kun; Meyerhoff, Mark E.
Journal of Materials Chemistry, 2012 , vol. 22, # 36 p. 18784 - 18787