2-甲基-1,4-丁二醇合成路线 (共 15 条)
反应条件
1: Na2S*2H2O View Scheme
参考文献
Whitehead et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3632
反应条件
in chloroform T=30°C; 4 h; Pseudomonas fluorescens lipase (PFL); var. times, also benzyl ether derivatives; Product distribution;
参考文献
Grisenti; Ferraboschi; Casati; Santaniello
Tetrahedron Asymmetry, 1993 , vol. 4, # 5 p. 997 - 1006
反应条件
1: Na2S*2H2O 2: m-CPBA View Scheme
参考文献
Della, Ernest W.; Graney, Sean D.
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3824 - 3835
反应条件
in chloroform T=30°C; 4 h; Pseudomonas fluorescens lipase (PFL); var. times, also benzyl ether derivatives; Product distribution;
参考文献
Grisenti; Ferraboschi; Casati; Santaniello
Tetrahedron Asymmetry, 1993 , vol. 4, # 5 p. 997 - 1006
参考文献
Faworsdi
Justus Liebigs Annalen der Chemie, 1907 , vol. 354, p. 362
Chem. Zentralbl., 1908 , vol. 79, # I p. 1041
反应条件
Nafion-H T=135°C; 5 h;
参考文献
Olah, George A.; Fung, Alexander P.; Malhotra, Ripudaman
Synthesis, 1981 , # 6 p. 474 - 476
参考文献
E.I. DU PONT DE NEMOURS AND COMPANY
Patent: EP790971 B1, 2001 ;
参考文献
Harries; Neresheimer
Justus Liebigs Annalen der Chemie, 1911 , vol. 383, p. 169
反应条件
triethylamine; 4-phenylbut-3-en-2-one; tris(triphenylphosphine)ruthenium(II) chloride in toluene T=110°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Ishii, Youichi; Osakada, Kohtaro; Ikariya, Takao; Saburi, Masahiko; Yoshikawa, Sadao
Journal of Organic Chemistry, 1986 , vol. 51, # 11 p. 2034 - 2039
反应条件
1: HBr / 140 - 145 °C
2: benzene
View Scheme
参考文献
Qudrat-i-Khuda; Ghosh
Journal of the Indian Chemical Society, 1940 , vol. 17, p. 19,24