反应条件
1: 98 percent / NaBH4 / tetrahydrofuran; methanol / 2 h 2: SOCl2 / benzene / 20 °C 3: dimethylsulfoxide; benzene / 2 h 4: 92 percent / 4N NaOH / ethanol / 20 h / Heating 5: SOCl2 / benzene / 2 h / 50 - 60 °C 6: 91 percent / benzene; pyridine / 20 °C 7: 85 percent / POCl3 / toluene / 3 h / Heating 8: 100 percent / NaBH4 / methanol / 0.25 h 9: 75 percent / Pd(OAc)2; PPh3; K2CO3 / toluene / 26 h / Heating 10: 87 percent / LiAlH4 / tetrahydrofuran / 0.75 h / Heating View Scheme
参考文献
Orito, Kazuhiko; Miyazawa, Mamoru; Kanbayashi, Ryo; Tokuda, Masao; Suginome, Hiroshi
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6583 - 6596
