4-(2,6-二苯基-4-吡啶基)-N,N-二甲基苯胺合成路线 （共 20 条）
反应条件
sodium hydrogensulfite; copper(I) bromide in dimethyl sulfoxide T=120°C; 2.5 h; Inert atmosphere;
参考文献
Ren, Zhi-Hui; Zhang, Zhi-Yuan; Yang, Bing-Qin; Wang, Yao-Yu; Guan, Zheng-Hui
Organic Letters, 2011 , vol. 13, # 19 p. 5394 - 5397
反应条件
ammonium hydroxide in acetone T=50°C; 2 h;
参考文献
Bak, Tomasz; Rasala, Danuta; Gawinecki, Ryszard
Organic Preparations and Procedures International, 1994 , vol. 26, # 1 p. 101 - 110
反应条件
2,4,6-trichloro-1,3,5-triazine; ammonium acetate; water T=130°C; 7 h; Neat (no solvent);
参考文献
Maleki, Behrooz; Azarifar, Davood; Veisi, Hojat; Hojati, Seyede Fatemeh; Salehabadi, Hafezeh; Yami, Razieh Nejat
Chinese Chemical Letters, 2010 , vol. 21, # 11 p. 1346 - 1349
反应条件
1-methylguanidine hydrochloride T=180°C; 0.0833333 h; Microwave irradiationneat (no solvent);
参考文献
Adib, Mehdi; Mohammadi, Bagher; Rahbari, Sahar; Mirzaei, Peiman
Chemistry Letters, 2008 , vol. 37, # 10 p. 1048 - 1049
反应条件
1: 3 h / 100 °C 2: sodium hydrogensulfite; copper(I) bromide / dimethyl sulfoxide / 2.5 h / 120 °C / Inert atmosphere View Scheme
参考文献
Ren, Zhi-Hui; Zhang, Zhi-Yuan; Yang, Bing-Qin; Wang, Yao-Yu; Guan, Zheng-Hui
Organic Letters, 2011 , vol. 13, # 19 p. 5394 - 5397
反应条件
toluene-4-sulfonic acid in xylene 48 h; Heating;
参考文献
Kakiuchi, Hidetaka; Kobayashi, Tomoshige; Kato, Hiroshi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 8 p. 2588 - 2589
反应条件
MgAl2O4; ammonium acetate in neat (no solvent) T=120°C; 3 h; Sealed tube; Mechanism;
参考文献
Safari, Javad; Zarnegar, Zohre; Borujeni, Mahmoud Borjian
Chemical Papers, 2013 , vol. 67, # 7 p. 688 - 695
参考文献
Weiss
Journal of the American Chemical Society, 1952 , vol. 74, p. 200
反应条件
1: 1.) conc. H2SO4, 2.) 70percent HClO4 / 1.) 100 deg C, 3 h, 2.) EtOH, overnight 2: 64 percent / 25percent aq. NH3 / acetone / 2 h / 50 °C View Scheme
参考文献
Bak, Tomasz; Rasala, Danuta; Gawinecki, Ryszard
Organic Preparations and Procedures International, 1994 , vol. 26, # 1 p. 101 - 110
反应条件
1: 1.) conc. H2SO4, 2.) 70percent HClO4 / 1.) 100 deg C, 3 h, 2.) EtOH, overnight 2: 64 percent / 25percent aq. NH3 / acetone / 2 h / 50 °C View Scheme
参考文献
Bak, Tomasz; Rasala, Danuta; Gawinecki, Ryszard
Organic Preparations and Procedures International, 1994 , vol. 26, # 1 p. 101 - 110
