反应条件
in tetrachloromethane
byproducts: NH4Br, S; passing NH3 through soln. of S2Br2 (10°C, 3 h), stirring for further 10 min; collection (filtration), stirring with water, drying (over CaCl2), extn.into dioxane, cooling (crystn.), evapn. of mother liquor, dissoln. of c ombined fractions in CCl4, stirring with Hg, filtration, evapn., crystn.(C6H6); elem. anal.;
参考文献
Padma, D. K.; Bhat, V. Subrahmanya; Murthy, A. R. Vansudeva
Inorganica Chimica Acta, 1976 , vol. 20, p. L53 - L54