2-O-(9-十八碳烯基)甘油合成路线 （共 5 条）
反应条件
boric acid trimethyl ester; boric acid T=100°C; 0.333333 h; Heating;
参考文献
Suhara, Yoshitomo; Takayama, Hiroaki; Nakane, Shinji; Miyashita, Tomoyuki; Waku, Keizo; Sugiura, Takayuki
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 7 p. 903 - 907
反应条件
1.1: KOH / toluene / 3 h / Heating 1.2: toluene / 6 h / Heating 2.1: 9.8 g / aq. HCl / methanol / 2 h / 80 °C View Scheme
参考文献
Joll, Cynthia A.; Mortimer, Bok-Cheng; Redgrave, Trevor G.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 8 p. 1445 - 1448
反应条件
hydrogenchloride in methanol 20 h; Heating;
参考文献
Joll, Cynthia A.; Mortimer, Bok-Cheng; Redgrave, Trevor G.; Stick, Robert V.
Australian Journal of Chemistry, 1990 , vol. 43, # 8 p. 1445 - 1448
反应条件
1: 31 percent / Ag2O; NBu4NI / dimethylformamide / 6 h / 90 °C 2: 52 percent / boric acid; trimethyl borate / 0.33 h / 100 °C / Heating View Scheme
参考文献
Suhara, Yoshitomo; Takayama, Hiroaki; Nakane, Shinji; Miyashita, Tomoyuki; Waku, Keizo; Sugiura, Takayuki
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 7 p. 903 - 907
反应条件
1: 80 percent / methyltriphenoxyphosphonium iodide / dimethylformamide / 0.33 h / 20 °C 2: 31 percent / Ag2O; NBu4NI / dimethylformamide / 6 h / 90 °C 3: 52 percent / boric acid; trimethyl borate / 0.33 h / 100 °C / Heating View Scheme
参考文献
Suhara, Yoshitomo; Takayama, Hiroaki; Nakane, Shinji; Miyashita, Tomoyuki; Waku, Keizo; Sugiura, Takayuki
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 7 p. 903 - 907
