N,N-二十二烷基甲基胺合成路线 (共 27 条)
反应条件
hydrogen; magnesium/copper (0.76 ratio) oxide catalyst with copper content 40percent by mass T=250°C; P=11251.1 Torr; 6 h; Autoclave; Product distribution / selectivity;
参考文献
Kao Corporation
Patent: EP1992608 A1, 2008 ;
Location in patent: Page/Page column 7-8 ;
反应条件
hydrogen; dimethyl amine; Cu/Cr Cu1800p catalyst in water T=250°C; P=11251.1 Torr; Inert atmosphereAutoclave; Product distribution / selectivity;
参考文献
Kao Corporation
Patent: US2010/179349 A1, 2010 ;
Location in patent: Page/Page column 8 ;
反应条件
hydrogen; Cu, Ni, Ru film catalyst containing thermosetting resin T=220°C; 6.7 h; Product distribution / selectivity;
参考文献
KAO CORPORATION
Patent: WO2006/109848 A1, 2006 ;
Location in patent: Page/Page column 14-15; 18 ;
反应条件
1: N,N-didodecylamine With formic acid in ethanol T=40°C; Inert atmosphere; 2: formaldehyd in ethanol T=82°C; Inert atmosphere; 3: With sodium hydroxide in ethanol; water T=20°C; Inert atmosphere;
参考文献
Tiecco, Matteo; Di Profio, Pietro; Germani, Raimondo; Savelli, Gianfranco
Nucleosides, Nucleotides and Nucleic Acids, 2009 , vol. 28, # 10 p. 911 - 923
反应条件
hydrogen; dimethyl amine; CuCr catalyst Cu0203 Engelhard T=250°C; P=3750.38 Torr; 24 - 720 h; Gas phase; Product distribution / selectivity;
参考文献
TAMINCO
Patent: WO2006/136204 A1, 2006 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; dimethyl amine; CuCr catalyst (Cu0203 Engelhard) T=250°C; P=3750.38 - 7500.75 Torr; 24 - 720 h; Product distribution / selectivity;
参考文献
TAMINCO
Patent: US2006/287556 A1, 2006 ;
Location in patent: Page/Page column 4,5 ;
参考文献
Westphal; Jerchel
Chemische Berichte, 1940 , vol. 73, p. 1007
反应条件
tris(triphenylphosphine)ruthenium(II) chloride T=180°C; 12 h;
参考文献
Arcelli, Antonio; Khai, Bui-The; Porzi, Gianni
Journal of Organometallic Chemistry, 1982 , vol. 235, # 1 p. 93 - 96
反应条件
hydrogen; copper-chromium powder; Titanium(IV) oxide T=250°C; P=50 Torr;
参考文献
Barrault; Brunet; Suppo-Essayem; Piccirilli; Guimon
JAOCS, Journal of the American Oil Chemists' Society, 1994 , vol. 71, # 11 p. 1231 - 1238
反应条件
ammonia; hydrogen; copper-chromium powder; Titanium(IV) oxide T=250°C; P=50 Torr;
参考文献
Barrault; Brunet; Suppo-Essayem; Piccirilli; Guimon
JAOCS, Journal of the American Oil Chemists' Society, 1994 , vol. 71, # 11 p. 1231 - 1238