N,N-二甲基甲酰胺-d1合成路线 （共 3 条）
反应条件
1: dimethyl amine With oxygen T=-153.16°C; 2: perdeuteroformaldehyde T=-153.16 - -98.16°C; chemoselective reaction;
参考文献
PRESIDENT AND FELLOWS OF HARVARD COLLEGE; MADIX, Robert, J.; ZHOU, Ling; XU, Bingjun; FRIEND, Cynthia, M.; FREYSCHLAG, Cassandra, G.
Patent: WO2011/91427 A1, 2011 ;
Location in patent: Page/Page column 11 ;
反应条件
triphenylmethane in benzene-d6 amine was added to a soln. in C6D6 in NMR tube for 5 min (Ar); not sepd., detected by NMR spectra;
参考文献
Ovchinnikov, Maxim V.; Guzei, Ilia A.; Angelici, Robert J.
Organometallics, 2001 , vol. 20, # 4 p. 691 - 696
反应条件
triethylamine 0.5 h;
参考文献
Bartmess, John E.; Caldwell, Gary; Rozeboom, Melvin D.
Journal of the American Chemical Society, 1983 , vol. 105, # 3 p. 340 - 344
