tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran
T=20°C;
参考文献
Hughes, Gregory; Wang, Changsheng; Batsanov, Andrei S.; Fern, Michael; Frank, Stephen; Bryce, Martin R.; Perepichka, Igor F.; Monkman, Andrew P.; Lyons, Benjamin P.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3069 - 3077
Hughes, Gregory; Wang, Changsheng; Batsanov, Andrei S.; Fern, Michael; Frank, Stephen; Bryce, Martin R.; Perepichka, Igor F.; Monkman, Andrew P.; Lyons, Benjamin P.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 17 p. 3069 - 3077
1: hydrogenchloride / methanol; dichloromethane / 1 h / 40 °C
2: sodium hydroxide; hydroxylamine-o-sulphonic acid / ethanol; water / 0.5 h / 60 °C
3: sodium periodate / dichloromethane; water / 12 h / 0 °C
4: 1,4-dioxane / 6 h / 22 °C
View Scheme
参考文献
Anderson, Erin D.; Boger, Dale L.
Journal of the American Chemical Society, 2011 , vol. 133, # 31 p. 12285 - 12292
