4-叔丁基-N,N-二甲基苯胺合成路线 (共 9 条)
反应条件
1.54H2O*Cl2Ni; ICy*HBF4 in tetrahydrofuran T=-10°C; Kumada coupling reaction; 1.5 h; Inert atmosphere;
参考文献
Joshi-Pangu, Amruta; Wang, Chao-Yuan; Biscoe, Mark R.
Journal of the American Chemical Society, 2011 , vol. 133, # 22 p. 8478 - 8481
反应条件
T=110°C; 2 h; in air;
参考文献
Li, Lan-Tao; Li, Hong-Ying; Xing, Li-Juan; Wen, Li-Juan; Wang, Peng; Wang, Bin
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 48 p. 9519 - 9522
反应条件
formic acid; iron(II) chloride heptahydrate; triethylamine T=150°C; 12 h;
参考文献
Jiang, Xue; Wang, Chao; Wei, Yawen; Xue, Dong; Liu, Zhaotie; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 58 - 63
反应条件
Pd(P(o-Tol)3)2 in benzene T=90°C; other tributyltin amides, var. palladium complexes; Product distributionMechanism;
参考文献
Hartwig, John F.; Richards, Steven; Baranano, David; Paul, Frederic
Journal of the American Chemical Society, 1996 , vol. 118, # 15 p. 3626 - 3633
反应条件
sodium cyanoborohydride; acetic acid Inert atmosphere;
参考文献
Chiranjeevi, Barreddi; Koyyada, Ganesh; Prabusreenivasan; Kumar, Vanaja; Sujitha, Pombala; Kumar, C. Ganesh; Sridhar; Shaik, Saida; Chandrasekharam, Malapaka
RSC Advances, 2013 , vol. 3, # 37 p. 16475 - 16485
反应条件
hydrogenchloride T=200 - 220°C; im Rohr;
参考文献
Malherbe
Chemische Berichte, 1919 , vol. 52, p. 322
参考文献
Davies; Hulbert
Journal of the Society of Chemical Industry, London, 1938 , vol. 57, p. 349
反应条件
in tetrahydrofuran T=0°C; Grignard reaction; Kinetics;
参考文献
Erdik, Ender; Uelhue, Selma Ates
Journal of Physical Organic Chemistry, 2007 , vol. 20, # 9 p. 671 - 676
反应条件
1-chloro-3-nitrobenzene in benzene
3 h; Irradiation; Yield given;
参考文献
Doepp, Dietrich; Heufer, Joerg
Tetrahedron Letters, 1982 , vol. 23, # 15 p. 1553 - 1556