1,1-双(溴甲基)环丙烷合成路线 （共 20 条）
反应条件
hydrogen bromide; phosphorus tribromide in dichloromethane 96 h;
参考文献
Evans, D. A.; Mitch, C. H.
Tetrahedron Letters, 1982 , vol. 23, # 3 p. 285 - 288
反应条件
hydrogen bromide; potassium carbonate in diethyl ether; pentane T=0°C; 0.333333 h; Irradiation;
参考文献
Zefirov, N. S.; Surmina, L. S.; Sadovaya, N. K.; Blokhin, A. V.; Tyurekhodzhayeva, M. A.; et al.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 11 p. 2002 - 2014
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 11 p. 2317 - 2333
反应条件
tetrachloromethane; bromine
参考文献
Applequist; Roberts
Journal of the American Chemical Society, 1956 , vol. 78, p. 874
参考文献
Applequist; Roberts
Journal of the American Chemical Society, 1956 , vol. 78, p. 874
反应条件
1: 75 percent / BH3 / tetrahydrofuran / Ambient temperature 2: 75 percent / PBr3, HBr / CH2Cl2 / 96 h View Scheme
参考文献
Evans, D. A.; Mitch, C. H.
Tetrahedron Letters, 1982 , vol. 23, # 3 p. 285 - 288
反应条件
1: K2CO3-solution 2: PBr3 / 140 °C / im Rohr View Scheme
参考文献
Zelinsky; Krawetz
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1876
Chemische Berichte, 1913 , vol. 46, p. 165
反应条件
bromine in tetrachloromethane 0.666667 h; Ambient temperatureIrradiation; Product distributionMechanism;
参考文献
Kennedy, Alan J.; Walton, John C.; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 751 - 757
反应条件
trichloromonobromomethane T=20°C; 60 h; Irradiation; Product distribution;
参考文献
Kennedy, Alan J.; Walton, John C.; Ingold, Keith U.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 751 - 757
参考文献
Applequist; Roberts
Journal of the American Chemical Society, 1956 , vol. 78, p. 874
反应条件
tri-n-butyl-tin hydride; tert-butyl hyponitrite in benzene T=45°C; 6 h; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 751 - 757
