2,2-二氯-1-(4-甲氧基苯基)乙酮合成路线 （共 16 条）
反应条件
palladium 10 on activated carbon; hydrogen in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 0.8 h; chemoselective reaction;
参考文献
Sawama, Yoshinari; Imanishi, Takahiro; Nakatani, Ryosuke; Fujiwara, Yuta; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2014 , vol. 70, # 30 p. 4540 - 4546
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione; copper(II) bis(trifluoromethanesulfonate) in chloroform 6 h; RefluxInert atmosphere;
参考文献
Jagdale, Arun R.; Chouthaiwale, Pandurang V.; Sudalai, Arumugam
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 10 p. 1424 - 1430
反应条件
in neat (no solvent) T=150°C; P=1 Torr; 0.0833333 h;
参考文献
Reutrakul, Vichai; Herunsalee, Kitivit
Tetrahedron Letters, 1983 , vol. 24, # 5 p. 527 - 530
反应条件
aluminium trichloride T=5 - 10°C; 3 h;
参考文献
Bandyopadhyay; Bagchi; Podder; Moitra
Journal of the Indian Chemical Society, 1989 , vol. 66, # 4 p. 239 - 240
反应条件
hydrogenchloride; potassium permanganate in acetonitrile T=60°C;
参考文献
Cheng, Sheng-Fan; Lin, Ching-Shan; Liu, Lilian Kao
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1997 , vol. 44, # 3 p. 309 - 312
反应条件
[BMIM(SO3H)][OTf]; N-chloro-succinimide T=70°C; 1.5 h; Green chemistry;
参考文献
Vrazic, Dejan; Jereb, Marjan; Laali, Kenneth K.; Stavber, Stojan
Molecules, 2013 , vol. 18, # 1 p. 74 - 96
反应条件
1: 83 percent / lithium diisopropylamide / tetrahydrofuran / 1 h / from -78 to -20 degC. 2: 98 percent / neat (no solvent) / 0.08 h / 150 °C / 1 Torr View Scheme
参考文献
Imanishi, Takahiro; Fujiwara, Yuta; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 771 - 776
反应条件
1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione in acetonitrile T=20°C; 0.75 h; Inert atmosphere;
参考文献
Chen, Zizhan; Zhou, Bin; Cai, Huihua; Zhu, Wei; Zou, Xinzhuo
Green Chemistry, 2009 , vol. 11, # 2 p. 275 - 278
反应条件
1.1: sodium dichromate; sulfuric acid / acetic acid / 0.17 h / 20 °C 1.2: 0.17 h 2.1: palladium 10 on activated carbon; hydrogen / N,N-dimethyl acetamide / 0.8 h / 25 °C / 760.05 Torr View Scheme
参考文献
Imanishi, Takahiro; Fujiwara, Yuta; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 5 p. 771 - 776
反应条件
manganese triacetate; ammonium chloride in acetic anhydride; acetic acid Heatingother substituted acetophenones, var. reagent, solvent, time; Product distribution;
参考文献
Kurosawa, Kazu; Yamaguchi, Katsutoshi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 6 p. 1757 - 1760
