H-ARG-VAL-OH合成路线 （共 12 条）
反应条件
palladium; acetic acid Hydrogenation;
参考文献
Zervas et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2878,2881
反应条件
hydrogen; palladium in methanol; water; acetic acid
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
1: triethylamine; chlorocarbonic acid isobutyl ester; CHCl3 / weiteres Reagens: Toluol; anschliessend Behandeln mit L-Valin-benzylester-toluol-4-sulfonat und Triaethylamin in CHCl3 2: palladium; methanol; acetic acid / Hydrogenation View Scheme
参考文献
Zervas et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 2878,2881
反应条件
1: PhSO3H / Heating 2: (i) Et3N, ClCO2Et, THF, (ii) /BRN= 2559321/ 3: H2 / Pd / methanol; acetic acid; H2O View Scheme
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
1: aq. NaOH 2: (i) Et3N, ClCO2Et, THF, (ii) /BRN= 2559321/ 3: H2 / Pd / methanol; acetic acid; H2O View Scheme
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
1: (i) Et3N, ClCO2Et, THF, (ii) /BRN= 2559321/ 2: H2 / Pd / methanol; acetic acid; H2O View Scheme
参考文献
Scopes,P.M. et al.
Journal of the Chemical Society, 1965 , p. 782 - 786
反应条件
1: (i) Et3N, ClCO2Et, THF, (ii) /BRN= 2559321/ 2: H2 / Pd / methanol; acetic acid; H2O View Scheme
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
1: NO2/HNO3, SO3/H2SO4 2: aq. NaOH 3: (i) Et3N, ClCO2Et, THF, (ii) /BRN= 2559321/ 4: H2 / Pd / methanol; acetic acid; H2O View Scheme
参考文献
Gibian,H.; Schroeder,E.
Justus Liebigs Annalen der Chemie, 1961 , vol. 642, p. 145 - 162
反应条件
magnesium sulphate heptahydrate; recombinant L-amino acid ligase RizA; ATP disodium salt; tri-(hydroxymethyl)-methylamine in water T=30°C; pH=8; 18 h; aq. buffer;
参考文献
Kino, Kuniki; Kotanaka, Yoichi; Arai, Toshinobu; Yagasaki, Makoto
Bioscience, Biotechnology and Biochemistry, 2009 , vol. 73, # 4 p. 901 - 907
反应条件
1: (i) ClCO2Et, Et3N, (ii) /BRN= 1721775/ 2: aq. NaOH 3: aq. HBr / acetic acid 4: H2SO4 / (electrochemical reduction) View Scheme
参考文献
Scopes,P.M. et al.
Journal of the Chemical Society, 1965 , p. 782 - 786
