3-甲基-1-苯基-2-丁酮合成路线 (共 74 条)
反应条件
gold(III) chloride; silver hexafluoroantimonate in 1,4-dioxane T=20°C; 0.0833333 h; regioselective reaction;
参考文献
Gudla, Vanajakshi; Balamurugan, Rengarajan
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5243 - 5247
反应条件
tri-n-butyltin methoxide; bis (triortho-tolylphosphine)palladium(II) chloride in toluene T=100°C; 5 h;
参考文献
Kosugi, Masanori; Hagiwara, Isao; Sumiya, Takashi; Migita, Toshihiko
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 344 - 345
反应条件
carbon monoxide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; selenium in tetrahydrofuran T=120°C; P=22800 Torr; 24 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 33, # 42 p. 6347 - 6350
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-45°C; 2 h;
参考文献
Wender, Paul A.; Erhardt, Jeanette M.; Letendre, Leo J.
Journal of the American Chemical Society, 1981 , vol. 103, # 8 p. 2114 - 2116
反应条件
chromium(VI) oxide - pyridine in dichloromethane
参考文献
Barentsen, Helma M.; Sieval, Alex B.; Cornelisse, Jan
Tetrahedron, 1995 , vol. 51, # 27 p. 7495 - 7520
反应条件
in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Journal of the American Chemical Society, , vol. 111, # 12 p. 4392 - 4398
反应条件
1: isopropylmagnesium chloride With indium(III) chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: carbon monoxide; benzyl bromide With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane T=60°C; 6 h;
参考文献
Lee, Sung Wook; Lee, Kooyeon; Seomoon, Dong; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Lee, Phil Ho
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4852 - 4855
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide; tert-butyl alcohol in tetrahydrofuran T=0°C;
参考文献
Hutton, Thomas K.; Muir, Kenneth; Procter, David J.
Organic Letters, 2002 , vol. 4, # 14 p. 2345 - 2347
反应条件
tetra-n-butylammonium tetrafluoroborate; NiBr2bipy in acetonitrile Ambient temperaturezinc rod as the anode, vitreous carbon gauze as the cathode, 0.1 A;
参考文献
Marzouk, H.; Rollin, Y.; Folest, J. C.; Nedelec, J. Y.; Perichon, J.
Journal of Organometallic Chemistry, 1989 , vol. 369, p. C47 - C50
反应条件
PhSeNa in ethanol 3 h; Ambient temperature;
参考文献
Satoh, Tsuyoshi; Kaneko, Youhei; Izawa, Takao; Sakata, Kiichi; Yamakawa, Koji
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 7 p. 1983 - 1990