1-甲基环己烷羰基氯化物合成路线 （共 18 条）
反应条件
aluminium trichloride
参考文献
Ismailov,A.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, # 10 p. 2196 - 2200
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2115 - 2120
反应条件
hydrogen; palladium on activated charcoal T=190°C;
参考文献
Puzitskii,K.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1968 , # 5 p. 1061 - 1063
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1968 , # 5 p. 1117 - 1120
反应条件
1: H2 / Pd-C / 190 °C 2: N2H4, KOH View Scheme
参考文献
Puzitskii,K.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1968 , # 5 p. 1061 - 1063
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1968 , # 5 p. 1117 - 1120
反应条件
1: pentane / 336 h / Ambient temperature 2: 76 percent / NaOH / 120 °C View Scheme
参考文献
Roesch, Wolfgang; Vogelbacher, Uwe; Allspach, Thomas; Regitz, Manfred
Journal of Organometallic Chemistry, 1986 , vol. 306, p. 39 - 54
反应条件
copper(l) chloride in diethyl ether
参考文献
Rouzaud,J. et al.
Bulletin de la Societe Chimique de France, 1965 , p. 2030 - 2037
参考文献
Charpentier-Morize,M. et al.
Bulletin de la Societe Chimique de France, 1962 , p. 273 - 282
反应条件
1: AcCl / CH2Cl2
2: Na2B4O7 / methanol
3: 600 °C / 14 Torr
View Scheme
参考文献
Karpf,M.; Dreiding,A.S.
Helvetica Chimica Acta, 1979 , vol. 62, p. 852 - 865
反应条件
aluminium trichloride
参考文献
Ismailov,A.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1971 , vol. 7, # 10 p. 2196 - 2200
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, # 10 p. 2115 - 2120
反应条件
ethylmagnesium bromide; ammonium chloride
1.) Et2O, reflux, 2h, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Clark, Brian J.; Grayshan, Roder; Miller, David D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2237 - 2240
反应条件
1: triethylamine / CHCl3
2: POCl3 / 0.5 h / 100 - 110 °C
3: 80.8 percent / 2N NaOH / ethanol / 0.25 h / 90 deg C bath
View Scheme
参考文献
Meguro; Tawada; Sugiyama; Fujita; Kawamatsu
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2840 - 2851
