1H-1,2,3-三氮唑合成路线 （共 105 条）
反应条件
caesium carbonate; copper(II) oxide; iron (III) acetylacetonate in N,N-dimethyl-formamide
T=90°C; 30 h;
参考文献
Taillefer, Marc; Xia, Ning; Ouali, Armelle
Angewandte Chemie - International Edition, 2007 , vol. 46, # 6 p. 934 - 936
反应条件
caesium carbonate; Fe(acac)3; copper(II) oxide in N,N-dimethyl-formamide
T=90°C; 30 h; sealed tube; Conversion of starting material;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S.); Ecole Nationale Superieure de Chimie de Montpellier
Patent: WO2008/4088 A2, 2008 ;
Location in patent: Page/Page column 49-50 ;
反应条件
copper(I) oxide; 1,10-phenanthroline; tetrabutyl ammonium fluoride
T=110 - 115°C; 48 h;
参考文献
Tang, Bo-Xiao; Guo, Sheng-Mei; Zhang, Man-Bo; Li, Jin-Heng
Synthesis, 2008 , # 11 p. 1707 - 1716
反应条件
tetrabutyl ammonium fluoride; iron(III) chloride; copper
T=50°C; 24 h;
参考文献
Song, Ren-Jie; Deng, Chen-Liang; Xie, Ye-Xiang; Li, Jin-Heng
Tetrahedron Letters, 2007 , vol. 48, # 44 p. 7845 - 7848
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=120°C; 5 h; Inert atmosphereSchlenk technique;
参考文献
Tian, Qingshan; Chen, Xianmin; Liu, Wei; Wang, Zechao; Shi, Suping; Kuang, Chunxiang
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 45 p. 7830 - 7833
反应条件
N-bromosuccinmide in isopropanol acetate
参考文献
Wang, Xiao-Jun; Zhang, Li; Krishnamurthy, Dhileepkumar; Senanayake, Chris H.; Wipf, Peter
Organic Letters, 2010 , vol. 12, # 20 p. 4632 - 4635
反应条件
copper(I) oxide; dipotassium hydrogenphosphate
T=145°C; 24 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2006/293304 A1, 2006 ;
Location in patent: Page/Page column 34 ;
反应条件
copper; potassium carbonate
T=20 - 160°C; 7 h;
参考文献
Wang, Tao; Zhang, Zhongxing; Meanwell, Nicholas A.; Kadow, John F.; Yin, Zhiwei; Xue, Qiufen May; Regueiro-Ren, Alicia; Matiskella, John D.; Ueda, Yasutsugu
Patent: US2004/110785 A1, 2004 ;
Location in patent: Page 212-213 ;
反应条件
copper; potassium carbonate
T=160°C; 7 h;
参考文献
Ueda, Yasutsugu; Connolly, Timothy P.; Kadow, John F.; Meanwell, Nicholas A.; Wang, Tao; Chen, Chung-Pin H.; Yeung, Kap-Sun; Zhang, Zhongxing; Leahy, David Kenneth; Pack, Shawn K.; Soundararajan, Nachimuthu; Sirard, Pierre; Levesque, Kathia; Thoraval, Dominique
Patent: US2005/209246 A1, 2005 ;
Location in patent: Page/Page column 32 ;
反应条件
1: in ethanol; water
Reflux;
2: With methanesulfonyl chloride; triethylamine in dichloromethane
T=-30 - 20°C;
参考文献
Kalisiak, Jaroslaw; Sharpless, K. Barry; Fokin, Valery V.
Organic Letters, 2008 , vol. 10, # 15 p. 3171 - 3174
