1-萘-1-基丁烷-1-酮合成路线 （共 14 条）
反应条件
1: in tetrahydrofuran; diethyl ether T=0 - 20°C; 17 h; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether; water
参考文献
PROSIDION LIMITED
Patent: WO2006/85118 A2, 2006 ;
Location in patent: Page/Page column 25-26 ;
WO 2006/085118 A2
反应条件
1: n-butyllithium 2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux View Scheme
参考文献
Hu, Bin; Meng, Meng; Jiang, Shanshan; Deng, Weiping
Chinese Journal of Chemistry, 2012 , vol. 30, # 6 p. 1289 - 1294
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate Reflux;
参考文献
Hu, Bin; Meng, Meng; Jiang, Shanshan; Deng, Weiping
Chinese Journal of Chemistry, 2012 , vol. 30, # 6 p. 1289 - 1294
反应条件
carbon disulfide; aluminium trichloride T=0°C;
参考文献
Caille
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1911 , vol. 153, p. 393
参考文献
Blicke; Maxwell
Journal of the American Chemical Society, 1939 , vol. 61, p. 1780
反应条件
toluene anschliessendes Behandeln mit Eis und NH4Cl und Erhitzen des Reaktionsprodukts mit wss. H2SO4;
参考文献
Nunn; Henze
Journal of Organic Chemistry, 1947 , vol. 12, p. 540
反应条件
sodium 1.) THF, 25 deg C, 2 h, 2.) room temperature, 8 h; Yield givenMultistep reaction;
参考文献
Periasamy, Mariappan; Rama Reddy, Malladi; Bharathi, Pandi
Synthetic Communications, 1999 , vol. 29, # 4 p. 677 - 683
反应条件
carbon disulfide; aluminium trichloride
参考文献
Rousset
Bulletin de la Societe Chimique de France, 1896 , vol. <3> 15, p. 61
参考文献
Cagniant; Cagniant
Bulletin de la Societe Chimique de France, 1958 , p. 1448,1457
参考文献
Lapkin; Ponomarewa; Pinegina
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 1365
Chem.Abstr., 1953 , p. 4861
