4-(二甲氨基)-2,3,5,6-四氟吡啶合成路线 （共 7 条）
反应条件
in ethanol; water Addition of a 25 percent aq. soln. of (CH3)2NH to C5F5N, dissolved in ethanol, at 0 °C.;
参考文献
Banks, R. E.; Burgess, J. E.; Cheng, W. M.; Haszeldine, R. N.
Journal of the Chemical Society, 1965 , p. 575 - 594
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
Full Text Show Details
Haszeldine, R. N.; Banks, R. E.
Patent: US3317542 , 1967 ;
C.A., 1968 , vol. 68, p. 59442
反应条件
in toluene T=20°C; 0.5 h; Inert atmosphereSchlenk technique;
参考文献
Samuel, Prinson P.; Singh, Amit Pratap; Sarish, Sankaranarayana Pillai; Matussek, Julia; Objartel, Ina; Roesky, Herbert W.; Stalke, Dietmar
Inorganic Chemistry, 2013 , vol. 52, # 3 p. 1544 - 1549
反应条件
in diethyl ether T=20°C; 12 h; Inert atmosphere;
参考文献
Jana, Anukul; Sarish, Sankaranarayana Pillai; Roesky, Herbert W.; Leusser, Dirk; Objartel, Ina; Stalke, Dietmar
Chemical Communications, 2011 , vol. 47, # 19 p. 5434 - 5436
反应条件
1: neat (no solvent) 2: water; ethanol View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
反应条件
2: steel wool / neat (no solvent) 3: water; ethanol View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
反应条件
1: neat (no solvent, gas phase) 2: neat (no solvent) 3: water; ethanol View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
反应条件
1: neat (no solvent) 2: water; ethanol View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
