2,3,5,6-四氟异烟酸合成路线 (共 12 条)
反应条件
1: neat (no solvent) 2: sulfolane 3: not given 4: sulfuric acid View Scheme
参考文献
F: PerFHalOrg.5, 4, page 115 - 148
反应条件
2: steel wool / neat (no solvent) 3: sulfolane 4: not given 5: sulfuric acid View Scheme
参考文献
F: PerFHalOrg.5, 4, page 115 - 148
反应条件
in tetrahydrofuran reaction at -10°C, 2 hours;;
参考文献
Journal of the Chemical Society, , p. 5040 - 5045
反应条件
in tetrahydrofuran reaction at -15°C, 3 hours, warming to 20°C, 1 hour;;
参考文献
Journal of the Chemical Society, , p. 5040 - 5045
反应条件
1: With ozone in ethyl acetate 2: With Pd-BaSO4; hydrogen
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 8 p. 541 - 547
反应条件
1: diethyl ether / -10 °C 2: ozone / ethyl acetate View Scheme
参考文献
Journal of Fluorine Chemistry, , vol. 132, # 8 p. 541 - 547
反应条件
1: sulfolane 2: not given 3: sulfuric acid View Scheme
参考文献
F: PerFHalOrg.5, 4, page 115 - 148
反应条件
1: neat (no solvent, gas phase) 2: neat (no solvent) 3: sulfolane 4: not given 5: sulfuric acid View Scheme
参考文献
F: PerFHalOrg.5, 4, page 115 - 148
反应条件
1: neat (no solvent) 2: sulfolane 3: not given 4: sulfuric acid View Scheme
参考文献
F: PerFHalOrg.5, 4, page 115 - 148
反应条件
in sulfuric acid Inlet of dry CO2 (-10 °C, 2 h) and addition of diluted H2SO4.;
参考文献
Journal of the Chemical Society, , p. 5040 - 5045
BE660873 , ;
C.A., , vol. 65, p. 7152