1-氨基-4-氯蒽-9,10-二酮合成路线 （共 50 条）
反应条件
potassium nitrate in water; acetonitrile
T=15 - 20°C; 1 h; other reagent, other solvent, other time; Product distribution;
参考文献
Galushko, A. M.; Dokunikhin, N. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 7 p. 1347 - 1357
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1539 - 1549
反应条件
air
1.) acetonitrile, room temp., 2 h ; 2.) acetonitrile, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Galushko, A. M.; Dokunikhin, N. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 7 p. 1347 - 1357
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1539 - 1549
参考文献
Gornostaev, L. M.; Es'kin, A. P.; Korniets, E. D.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2093 - 2096
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2344 - 2346
反应条件
durch Chlorierung und Entacetylierung;
参考文献
Bad. Anilin- u. Sodaf.
Patent: DE199758 ;
参考文献
Bayer and Co.
Patent: DE206536 ;
反应条件
zinc dinitrate; air in water; acetonitrile
6 h; other reagent, other solvent, other time; Product distribution;
参考文献
Galushko, A. M.; Dokunikhin, N. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 7 p. 1347 - 1357
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1539 - 1549
反应条件
in dimethyl sulfoxide
T=25°C; Equilibrium constant;
参考文献
Os'kina, I. A.; Vlasov, V. M.; Terekhova, M. I.; Petrov, E. S.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.1 p. 2041 - 2044
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2261 - 2265
反应条件
1: 1) amyl nitrite 2) NaN3 / 1)acetic acid, room temperature 2) 30 min
2: toluene / 2 h / Heating
3: 70.5 percent / dimethylformamide / 2 h / 80 °C
View Scheme
参考文献
Gornostaev, L. M.; Zeibert, G. F.; Zolotareva, G. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 7 p. 704 - 707
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , # 7 p. 912 - 915
参考文献
Bayer and Co.
Patent: DE225232 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 9, p. 1199
反应条件
aluminium trichloride
Ambient temperature;
参考文献
Philip, George; Nabar, U. T.; Kanetkar, V. R.; Sunthankar, S. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 808 - 811
