1-氨基-4-氯蒽-9,10-二酮合成路线 （共 50 条）
反应条件
aluminium trichloride in nitrobenzene Ambient temperature;
参考文献
Philip, George; Nabar, U. T.; Kanetkar, V. R.; Sunthankar, S. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. <B> 22, # 8 p. 808 - 811
反应条件
[Cu(CH3CN)4]BF4 in acetonitrile T=70°C; Rate constantMechanism;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1789 - 1796
反应条件
propan-1-ol; 2-[2-(2-methoxy-ethoxy)-ethoxy]-ethanol; sodium hydride 1.) THF, 0.5 h, 2.) THF, reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Boldt, Peter; Zippel, Stephan; Haucke, Gerd
Journal of Chemical Research, Miniprint, 1997 , # 11 p. 2318 - 2346
反应条件
2-[2-(2-methoxy-ethoxy)-ethoxy]-ethanol; sodium hydride 1.) THF, 0.5 h, 2.) THF, reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Boldt, Peter; Zippel, Stephan; Haucke, Gerd
Journal of Chemical Research, Miniprint, 1997 , # 11 p. 2318 - 2346
反应条件
sodium hydride 1.) THF, 0.5 h, 2.) THF, reflux, 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Boldt, Peter; Zippel, Stephan; Haucke, Gerd
Journal of Chemical Research, Miniprint, 1997 , # 11 p. 2318 - 2346
反应条件
in dimethyl sulfoxide T=25°C; Equilibrium constant;
参考文献
Os'kina, I. A.; Vlasov, V. M.; Terekhova, M. I.; Petrov, E. S.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 11.1 p. 2041 - 2044
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 11 p. 2261 - 2265
反应条件
hydrogenchloride in acetic acid
Heating;
参考文献
Gornostaev, L. M.; Sakilidi, V. T.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 3 p. 562 - 565
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 3 p. 642 - 645
反应条件
hydrogenchloride in acetic acid
Heating;
参考文献
Gornostaev, L. M.; Sakilidi, V. T.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1980 , vol. 16, # 11 p. 1112 - 1114
Khimiya Geterotsiklicheskikh Soedinenii, 1980 , vol. 16, # 11 p. 1471 - 1473
反应条件
in sulfolane
T=130°C; 2 h;
参考文献
Kargina; Gornostaev; Nefedov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 1 p. 70 - 77
Zh. Org. Khim., 2013 , vol. 49, # 1 p. 79 - 85,7
