三环[3.1.1.0(6,7)]庚烷合成路线 （共 14 条）
反应条件
in benzene T=10°C; 7 h; PhotolysisInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 17 p. 2811 - 2817
反应条件
hydrogen; palladium on activated charcoal in pentane T=17°C; 0.05 h; the formed intermediates are detected with 1H-NMR-spectroscopy; Product distribution;
参考文献
Stahl, Karl-Johannes; Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1474 - 1484
反应条件
N-bromosuccinmide; triethylamine in water; acetone T=20°C; 3.5 h;
参考文献
Chemische Berichte, , vol. 127, # 2 p. 381 - 392
反应条件
hydrogen; palladium on activated charcoal in pentane T=17°C; 0.166667 h; the formed products are detected with gas chromatography; Product distribution;
参考文献
Stahl, Karl-Johannes; Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1474 - 1484
反应条件
hydrogen; palladium on activated charcoal in pentane T=17°C; 0.166667 h; the formed products are detected with gas chromatography; Product distribution;
参考文献
Stahl, Karl-Johannes; Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1474 - 1484
反应条件
hydrogen; palladium on activated charcoal in pentane T=17°C; 0.05 h; the formed intermediates are detected with 1H-NMR-spectroscopy; Product distribution;
参考文献
Stahl, Karl-Johannes; Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1474 - 1484
反应条件
hydrogen; palladium on activated charcoal in pentane T=17°C; 0.05 h; the formed intermediates are detected with 1H-NMR-spectroscopy; Product distribution;
参考文献
Stahl, Karl-Johannes; Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1474 - 1484
反应条件
1,4-dioxane; n-butyllithium; magnesium bromide; Cl2Ni(1,2-bis(diphenylphosphino)ethane) 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hashmi, A. Stephen K.; Vollmer, Antje; Szeimies, Guenter
Liebigs Annalen, 1995 , # 3 p. 471 - 476
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1.) RT, 2.) RT; Yield given. Multistep reaction;
参考文献
Koptelov, Yu. B.; Kostikov, R. R.; Molchanov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 12 p. 2181 - 2185
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 12 p. 2518 - 2523
反应条件
bromine in pentane T=-78°C; Further byproducts given;
参考文献
Xu; Miebach; Brinker; Smith
Tetrahedron Letters, 1991 , vol. 32, # 35 p. 4461 - 4464
