N-(4-氯-苯基)-苯酰胺合成路线 （共 91 条）
反应条件
1: nitric acid / -15 °C 2: sulfuric acid View Scheme
参考文献
van Horssen
Recueil des Travaux Chimiques des Pays-Bas, 1936 , vol. 55, p. 245,251
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in nitromethane
0.166667 h; MillingGreen chemistry;
参考文献
Strukil, Vjekoslav; Bartolec, Boris; Portada, Tomislav; Dilovic, Ivica; Halasz, Ivan; Margetic, Davor
Chemical Communications, 2012 , vol. 48, # 99 p. 12100 - 12102
反应条件
1: iodobenzene; 4-chloro-aniline With sodium carbonate in water
0.166667 h; Autoclave;
2: carbon dioxide in water
T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Revankar, Santosh A.; Khedkar, Mayur V.; Bhanage, Bhalchandra M.
Catalysis Today, 2012 , vol. 198, # 1 p. 148 - 153
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
反应条件
1: 4-chloro-aniline With C30H60Li4N8 in diethyl ether
0.5 h; Inert atmosphereSchlenk technique;
2: benzaldehyde in diethyl ether
T=20°C; 3 h; Inert atmosphereSchlenk technique;
参考文献
Guo, Zhiqiang; Liu, Qiao; Wei, Xuehong; Zhang, Yongbin; Tong, Hongbo; Chao, Jianbin; Guo, Jianping; Liu, Diansheng
Organometallics, 2013 , vol. 32, # 16 p. 4677 - 4683
反应条件
1,4-diaza-bicyclo[2.2.2]octane; bicycloheptadienemolybdenunim tetracarbonyl; tetrabutylammomium bromide in diethylene glycol dimethyl ether
T=140°C; 1.25 h;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Motevalli, Somayeh; Talebi, Mohsen
Tetrahedron, 2013 , vol. 69, # 1 p. 418 - 426
反应条件
sodium periodate; sulfuric acid; sodium lauryl sulfate; acetic acid; sodium chloride in water
T=25°C; 2 h;
参考文献
Mahajan, Tanu; Kumar, Lalit; Dwivedi, K.; Agarwal, D. D.
Synthetic Communications, 2012 , vol. 42, # 24 p. 3655 - 3663,9
反应条件
copper(I) oxide; water; caesium carbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate; sodium hydroxide; N-methyl-2-(methylamino)ethylamine
T=100°C; 12 h; Inert atmosphereSealed tube;
参考文献
Wang, Jichao; Yin, Xinchi; Wu, Jun; Wu, Datong; Pan, Yuanjiang
Tetrahedron, 2013 , vol. 69, # 48 p. 10463 - 10469
反应条件
K3PO4*3H2O; N-methyl-2-(methylamino)ethylamine in toluene
T=110°C; 10 h; Inert atmosphere;
参考文献
Yao, Zijian; Wei, Xianwen
Chinese Journal of Chemistry, 2010 , vol. 28, # 11 p. 2260 - 2268
反应条件
oxygen; lithium hydroxide hydrate in water
T=50°C; 12 h;
参考文献
Wang, Ye; Zhu, Dapeng; Tang, Lin; Wang, Sujing; Wang, Zhiyong
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8917 - 8921
