(Z)-氧代环十七碳-8-烯-2-酮合成路线 （共 7 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; triethylamine in acetone 6 h; Ambient temperature;
参考文献
Venkataraman, K.; Wagle, D. R.
Tetrahedron Letters, 1980 , vol. 21, p. 1893 - 1896
反应条件
1: 83 percent / 4-dimethylaminopyridine N-oxide; 2-methyl-6-nitrobenzoic anhydride; Et3N / CH2Cl2; tetrahydrofuran / 1 h / 20 °C 2: 91 percent / DMAP / toluene / 4 h / 130 °C 3: 87 percent / P(OMe)3 / 25 h / 140 °C View Scheme
参考文献
Villemin, Didier
Synthesis, 1987 , # 2 p. 154 - 155
反应条件
1: 91 percent / DMAP / toluene / 4 h / 130 °C 2: 87 percent / P(OMe)3 / 25 h / 140 °C View Scheme
参考文献
Shiina, Isamu; Hashizume, Minako
Tetrahedron, 2006 , vol. 62, # 33 p. 7934 - 7939
反应条件
1: 85 percent / PPh3, CCl4 / Heating 2: 400 mg / aq. NaOH / 4 h 3: 65 percent / K2CO3 / dimethylsulfoxide / 1 h / 100 °C View Scheme
参考文献
Subramanian; Passey, Sarita
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1998 , vol. 37, # 1 p. 23 - 27
反应条件
acetic anhydride 18 h; Heating; Yield given;
参考文献
Villemin, Didier
Synthesis, 1987 , # 2 p. 154 - 155
反应条件
(i) H2, PtO2, EtOH, (ii) N2H4*H2O; Multistep reaction;
参考文献
Allen,C.F.H.; Weismann Magder,E.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 349 - 360
反应条件
hydrogen; palladium on activated charcoal in diethyl ether P=760 Torr;
参考文献
Villemin, Didier
Synthesis, 1987 , # 2 p. 154 - 155
