反应条件
diphenyl diselenide in benzene
byproducts: Hg(SePh)2; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhSeSePh (1.2 equiv) in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 2.5h);; filtration; solvent removed (vacuum); yield detd. by GLC after aq. Na2S2O3/CH2Cl2 extn.; n-BuSePh analysed by (1)H NMR, GLC and GCMS;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538