7-氮杂双环[4.1.0]庚烷合成路线 (共 32 条)
反应条件
1.1: 50 percent / trifluoromethanesulfonic acid / CH2Cl2 / 24 h / 20 °C
2.1: (D)-tartaric acid / H2O / 80 °C
2.2: 65 percent / aq. NaOH
View Scheme
参考文献
Caiazzo, Aldo; Dalili, Shadi; Yudin, Andrei K.
Organic Letters, 2002 , vol. 4, # 15 p. 2597 - 2600
反应条件
triethylamine in diethyl ether
T=0°C; 1.5 h;
参考文献
Ekegren, Jenny K.; Roth, Peter; Kaellstroem, Klas; Tarnai, Tibor; Andersson, Pher G.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 2 p. 358 - 366