1H-苯并三唑-1-甲醇合成路线 (共 47 条)
反应条件
in water T=25°C; 0.0833333 h;
参考文献
Le Borgne, Marc; Na, Young Min; Pagniez, Fabrice; Le Baut, Guillaume; Le Pape, Patrice; Abdala, Hiam
Patent: US2004/67998 A1, 2004 ;
Location in patent: Page/Page column 24 ;
反应条件
1: aniline With hydrogenchloride; sodium nitrite in water 2: 4-(1H-benzo[1,2,3]triazol-1-yl)-3-(2-phenylhydrazono)butan-2-one With sodium acetate in ethanol T=20°C;
参考文献
Al-Mousawi, Saleh M.; Moustafa, Moustafa Sherief; Elnagdi, Mohamed Hilmy
Heterocycles, 2008 , vol. 75, # 9 p. 2201 - 2211
反应条件
tetrahydrofuran; lithium aluminium tetrahydride
参考文献
Gaylord; Kay
Journal of Organic Chemistry, 1958 , vol. 23, p. 1574
反应条件
in acetone T=20°C; 24 h;
参考文献
Chen, Shuo-Ping; Hu, Le; Zhang, Yu-Qin; Deng, Pu; Li, Cong; Chen, Xi; Yuan, Liang-Jie
Chemical Communications, 2012 , vol. 48, # 4 p. 552 - 554
反应条件
in benzene-d6 ΔG0; also reaction with other carbonyl compounds; Equilibrium constantThermodynamic data;
参考文献
Katritzky, Alan R.; Perumal, Subbu; Savage, G. Paul
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 6 p. 921 - 924
参考文献
Gaylord; Kay
Journal of Organic Chemistry, 1958 , vol. 23, p. 1574
反应条件
1: SOCl2 / toluene / 2 h / Heating 2: 87 percent / toluene; methanol / 2 h / Heating View Scheme
参考文献
Dumas, Aaron M.; Bode, Jeffrey W.
Organic Letters, 2012 , vol. 14, # 8 p. 2138 - 2141
反应条件
in toluene 24 h; Heating;
参考文献
Katritzky, Alan R.; Drewniak, Malgorzata
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2339 - 2344
反应条件
toluene-4-sulfonic acid in toluene 5 h; Heating;
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Chemische Berichte, 1991 , vol. 124, # 8 p. 1819 - 1826
反应条件
toluene-4-sulfonic acid in toluene 1 h; Heating;
参考文献
Katritzky, Alan R.; Lan, Xiangfu; Lam, Jamshed N.
Chemische Berichte, 1991 , vol. 124, # 8 p. 1819 - 1826