4-(苯基磺酰基)苯甲腈合成路线 （共 18 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 16 h;
参考文献
ZALICUS PHARMACEUTICALS LTD.; PAJOUHESH, Hassan, A.; HOLLAND, Richard; ZHANG, Lingyun; PAJOUHESH, Hossein, O.; LAMONTAGNE, Jason; WHELAN, Brendan; SHORT, Glenn, F., III.; ROMERO, Donna, L.
Patent: WO2013/131018 A1, 2013 ;
Location in patent: Page/Page column 54 ;
反应条件
in dimethyl sulfoxide T=130°C; 16 h;
参考文献
Ulman, Abraham; Urankar, Edward
Journal of Organic Chemistry, 1989 , vol. 54, # 19 p. 4691 - 4692
反应条件
n-Bu4N+CN- in dimethyl sulfoxide 1 h; Ambient temperatureIrradiationCPE on Pt cathode with n-Bu4N(1+)BF4(1-);
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'erba, Carlo
Tetrahedron, 1987 , vol. 43, # 20 p. 4625 - 4634
反应条件
copper(l) iodide in dimethyl sulfoxide 48 h; Heating;
参考文献
Bian, Ming; Xu, Fada; Ma, Cheng
Synthesis, 2007 , # 19 p. 2951 - 2956
反应条件
in dimethyl sulfoxide 1 h; Ambient temperatureIrradiationCPE on Pt cathode with n-Bu4N(1+)BF4(1-);
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'erba, Carlo
Tetrahedron, 1987 , vol. 43, # 20 p. 4625 - 4634
反应条件
1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 160 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C View Scheme
参考文献
ZALICUS PHARMACEUTICALS LTD.; PAJOUHESH, Hassan, A.; HOLLAND, Richard; ZHANG, Lingyun; PAJOUHESH, Hossein, O.; LAMONTAGNE, Jason; WHELAN, Brendan; SHORT, Glenn, F., III.; ROMERO, Donna, L.
Patent: WO2013/131018 A1, 2013 ;
反应条件
1: potassium tert-butylate / N,N-dimethyl-formamide / 0.5 h / 160 °C 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 16 h / 20 °C View Scheme
参考文献
ZALICUS PHARMACEUTICALS LTD.; PAJOUHESH, Hassan, A.; HOLLAND, Richard; ZHANG, Lingyun; PAJOUHESH, Hossein, O.; LAMONTAGNE, Jason; WHELAN, Brendan; SHORT, Glenn, F., III.; ROMERO, Donna, L.
Patent: WO2013/131018 A1, 2013 ;
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Kornblum,N. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 1560 - 1564
参考文献
Cymerman; Koebner; Short
Journal of the Chemical Society, 1948 , p. 381
Full Text Show Details
Oxley et al.
Journal of the Chemical Society, 1946 , p. 763,766
反应条件
chloroform; trichlorophosphate
参考文献
Fuller; Tonkin; Walker
Journal of the Chemical Society, 1945 , p. 633,639
