N-(叔丁基)-对甲苯磺酰胺合成路线 （共 28 条）
反应条件
1: 4-methyl N-t-butylbenzenesulfonamide With n-butyllithium in tetrahydrofuran T=-78 - -20°C; 4 h; Inert atmosphere; 2: tri-isopropoxy-borane in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; 3: With hydrogenchloride in tetrahydrofuran; water Inert atmosphere;
参考文献
Liu, Jie; Liu, Qin; Yang, Xue; Xu, Shengtao; Zhang, Hengyuan; Bai, Renren; Yao, Hequan; Jiang, Jieyun; Shen, Mingqin; Wu, Xiaoming; Xu, Jinyi
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 24 p. 7742 - 7751
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=50°C; 3 h;
参考文献
Mahalingam; Wu, Xiongyu; Wan, Yiqian; Alterman, Mathias
Synthetic Communications, 2005 , vol. 35, # 3 p. 417 - 425
反应条件
trifluorormethanesulfonic acid in toluene
T=120°C; 22 h;
参考文献
Shi, Wei; Bai, Chun-Mei; Zhu, Kai; Cui, Dong-Mei; Zhang, Chen
Tetrahedron, 2014 , vol. 70, # 2 p. 434 - 438
反应条件
tetraethylammonium p-toluenesulfonate in methanol
Electrochemical reactionreticulated vitreous carbon anode; Pt cathode;
参考文献
D'Oca, Marcelo G. Montes; Russowsky, Dennis; Canto, Karen; Gressler, Tanara; Goncalves, Reinaldo S.
Organic Letters, 2002 , vol. 4, # 10 p. 1763 - 1766
反应条件
lithium hexamethyldisilazane in tetrahydrofuran
T=50°C; 18 h;
参考文献
Wilden, Jonathan D.; Geldeard, Lynsey; Lee, Chieh C.; Judd, Duncan B.; Caddick, Stephen
Chemical Communications, 2007 , # 10 p. 1074 - 1076
反应条件
water in dichloromethane
T=20°C; 0.333333 h;
参考文献
Shaabani, Ahmad; Soleimani, Ebrahim; Hossein Rezayan, Ali
Tetrahedron Letters, 2007 , vol. 48, # 12 p. 2185 - 2188
反应条件
triethylamine in tetrahydrofuran
T=0 - 20°C;
参考文献
Born, Karolin; Doye, Sven
European Journal of Organic Chemistry, 2012 , # 4 p. 764 - 771
反应条件
[2,2']bipyridinyl; copper(l) iodide; oxygen in dimethyl sulfoxide
T=60°C; 24 h;
参考文献
Taniguchi, Nobukazu
European Journal of Organic Chemistry, 2010 , # 14 p. 2670 - 2673
反应条件
ethyldimethylsilane; (Ace)Ru3(CO)7 in dichloromethane
T=20°C; 6 h; Inert atmosphere;
参考文献
Nishikata, Takashi; Nagashima, Hideo
Angewandte Chemie - International Edition, 2012 , vol. 51, # 22 p. 5363 - 5366
反应条件
copper(ll) bromide in dimethyl sulfoxide
T=100°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Tang, Xiaodong; Huang, Liangbin; Qi, Chaorong; Wu, Xia; Wu, Wanqing; Jiang, Huanfeng
Chemical Communications, 2013 , vol. 49, # 54 p. 6102 - 6104
